Then add an mixture of sulfuric acid and nitric acid drop wise to solution while on ice and continuously mixing, mixture is 2 mL sulfuric acid and 2 mL nitric acid. Continue to swirl mixture in ice for two minute and then let it sit out of the ice for 15 minutes. Once at room temperature pour solution into a beaker with 4g of crushed ice and allow product to solidify. Then separate product with Hirsch funnel and wash solid with cold water and cold methanol. Then weigh the crude product and recrystallize it with and equal amount of methanol and slowly cool to form pure crystals. Lastly, filter out product, weigh it, calculate percent yield, melting point and conduct a proton and carbon
Then add an mixture of sulfuric acid and nitric acid drop wise to solution while on ice and continuously mixing, mixture is 2 mL sulfuric acid and 2 mL nitric acid. Continue to swirl mixture in ice for two minute and then let it sit out of the ice for 15 minutes. Once at room temperature pour solution into a beaker with 4g of crushed ice and allow product to solidify. Then separate product with Hirsch funnel and wash solid with cold water and cold methanol. Then weigh the crude product and recrystallize it with and equal amount of methanol and slowly cool to form pure crystals. Lastly, filter out product, weigh it, calculate percent yield, melting point and conduct a proton and carbon