In the Acid-Catalyzed Hydration of norbornene, water and sulfuric acid were added to the C=C double bond to form norborneol. Sulfuric acid acted as a catalyst, where it was not consumed in the reaction and helped to propel the reaction forward, as it was vital in forming hydronium ion and breaking the double bond. Both the products endo-norborneol and exo-norborneol were synthesized; however regioselectivity and stereoselectivity played a role as to which product was more preferred and whether the equatorial or axial orientation of the hydroxy group was favored. The setup of the Cold-Finger, and the ability of norborneol to sublime readily allowed for the purification of the crude product to obtain the diastereomeric products exo- and endo-norborneol.…
1. a. My data demonstrated the law of conservation of mass in part 5 of the experiment, dissolving sugar in water. The law of conservation mass states that matter cannot be created or destroyed by can enter or leave the system. The system’s change in mass was 0.00 grams, resulting in support of this statement.…
For this experiment, a group was employed by the Environmental Protection Agency as analytical chemists. Their goal was to identify an unknown compound that has been discovered in a landfill in their hometown. Once they identified the compound, they would then have to determine both the chemical and physical properties of the compound in order to inform the townspeople of any potential dangers. During the first week of lab, the group was given a small bottle containing an unknown white crystal-like substance.…
There may have been errors in the lab that may have affected the results of the lab. There may have been mistakes: a person may have not measured the substances correctly while retrieving the liquids in the graduated cylinder, or not have been watching the conductivity probe while the group was measuring the electrolyte solution. Along with these, there is also the issue of timing the testing incorrectly. Adding onto this, there may have been a slight spill where the accurate amount of the substance being used was not completely added into the water for testing.…
Lab 4 in Chem 115 has three parts all calculating density. In part one, a 100 mL beaker, a volumetric pipet, and an analytical scale were obtained. To begin, the mass of the beaker was taken using an analytical scale. Then, 10.0 mL of an unknown liquid was transfered to the beaker using the volumetric pipet. Next, the mass of the beaker and liqiud was recorded along with the letter identifying the unknown liquid.…
Nettie Stauts January 26, 2018 CDT-2413 Module 1 Lab Parents Perspective: The parents were apprehensive, but eager, entering their son Luke in a child care program. They were getting early intervention home-centered services in which Luke had progressed with assistance from his therapist and babysitter. He lacked social developmental skills and they heard about inclusion although unfamiliar with the concept. They were adapted interacting with Luke through gestures and augmentative communication devices yet anxious about his communication in the classroom.…
Given an unknown compound in container 3, solubility tests, cation tests, anion tests, and conductivity tests can be used to determine the various properties of the unknown to then make a positive identification of the unknown. These results will not only show chemical and physical properties but also what the unknown compound might react with to form other compounds. After performing the four anion tests, a positive identification was able to be made showing that the unknown compound contained a chloride ion since a white precipitate was formed from the reaction (Table 1). The sulfate, nitrate, and carbonate tests all yielded negative results when no precipitate was formed. The reaction of the chloride anion is as follows: Cl-…
Experiment 5 Synthesis and NMR Spectroscopy of ethyl cinnamate Introduction: Wittig reactions involve the stereoselective synthesis of olefins from phosphonium ylides and aldehydes or ketones, where the carbonyl bond is converted to an alkene double bond.1 The variety of suitable reagents and the relatively mild experimental conditions facilitate their industrial applications, such as the synthesis of epoxides, esters, carotenoids and vitamin A.2,3 Specifically, the ester ethyl cinnamate is used as a flavouring agent and in perfumes. The diastereomers of the alkene are distinguished through Proton Nuclear Magnetic Resonance (1H NMR) spectroscopy, where the coupling constants of alkenyl protons are different for (E) and (Z) isomers.4…
After starting with 30 mL of an unknown mixture of two solvents, fractional distillation and gas chromatography were used to identify the unknowns as acetone and toluene in a 1 to 2.04 ratio of acetone to toluene. Fractional distillation was first used to separate the unknown mixture into its components based on boiling point. Distillation refers to the method of separating components of a mixture through heating and cooling. Simple distillation, which is especially useful in the separation of less-volatile substances from volatile substances, such as sugar from water, can be used to separate a liquid-liquid mixture if the boiling points of the component liquids differ by more than 40-50°C. A plot of temperature versus volume for a simple…
One important aspect of organic chemistry is the synthesis of new compounds. It is also important for chemists to understand how to perform certain techniques, such as extraction and distillation, to produce the new products, which are usually drugs and cures for illnesses. In this experiment, n-butyl bromide was produced. n-Butyl bromide is an alkyl halide, which are usually synthesized by an alcohol and an acid. In the case of n-butyl bromide, n-butyl alcohol was used along with sodium bromide and sulfuric acid.…
In this equation, x and y denotes the number of moles of RE and Mn atoms per formula unit of the structure, respectively. The RE and Mn represent the theoretical magnetic moment of trivalent free RE3+ ions and divalent Mn2+ ions respectively. The experimental values of total magnetic moments were found to be smaller than the calculated values (Table xyz). The crystal field effects can lead to lower value of magnetic moments for RE3+ ions in these compositions as compared to free RE3+ ions, which in turn could lower the total magnetic moment of these compositions. This discrepancy in the total magnetic moment values could also be due to the presence of secondary phases in these samples.…
In Anastasia Toufexis’ “Love: The Right Chemistry,” Toufexis uses 3 different types of diction. The first 2 ways she uses diction is to dehumanize our emotions about ourselves and the way we see love, only to personalize those same emotions in the end. The last way she uses diction is to build a sense of trust. In the beginning, Toufexis uses diction to refine the way we see ourselves but ultimately changes this emotion in the end.…
Slime is made by mixing together borax, glue, and water. Depending on the amount of borax added to the mixture will determine the density of the slime. For our experiment in class the independent variable was the borax. The dependent variable was slime. The control group was glue.…
Benzocaine was synthesized from p-toluidine in a four step synthesis. Each intermediate product, including N-acetyl-p-toluidine, p-acetamidobenzoic acid, and p-aminobenzoic acid, was checked for yield, presence, and purity through weighing, taking IR and NMR spectrums, and determining the melting point. Thin Layer Chromatography was used to ensure the completion of the final reaction from p-aminobenzoic acid to benzocaine. The yield of the first step from p-toluidine to N-acetyl-p-toluidine was 91.9%. The yield of the second step from N-acetyl-p-toluidine to p-acetamidobenzoic acid was 49.85% The yield of the third step from p-acetamidobenzoic acid to p-aminobenzoic acid was 32.49%, which was not enough to continue so some product was borrowed…
A mixture of 5.0 mL concentrated nitric acid and 5.0 mL concentrated sulfuric acid was prepared in a 100-mL Erlenmeyer flask and was placed into a water bath to cool to room temperature. 3.93 grams of bromobenzene was added to the solution over a period of 10 minutes with constant mixing. After all of the bromobenzene is added, the mixture was heated with a hot water bath for 30 minutes. The flask was cooled to room temperature and then poured into 50 mL of ice-cold water in a 200 mL beaker. The crude product was isolated by vacuum filtration and then washed with cold water.…